This article is only available in the PDF format. Download the PDF to view the article, as well as its associated figures and tables.
To the Editor:
—I believe I have found a simpler method for preparing dichloramin-T than that described on the packages put out by the pharmaceutical houses. My method is:Weigh out amount of powdered dichloramin-T, place in mortar and rub up with small amount of chloroform (carbon tetrachlorid may be used) until all is dissolved, then add chlorcosane to the dissolved dichloramin-T. The chloroform is easily evaporated and thus leaves the dichloramin in solution in the solvent. By this method can be prepared a fresh solution of dichloramin-T in a few minutes, whereas the heat and cold methods take a much longer time. In the heat method, there is danger of overheating, in which a precipitation is caused, which renders the dichloramin-T useless and very irritating.
—We can see no advantage over the heat method, if the chloroform or carbon tetrachlorid must be removed by evaporation. However, the use
Anderson VJ. PREPARATION OF DICHLORAMIN-T. JAMA. 1919;73(20):1544. doi:10.1001/jama.1919.02610460062029
Customize your JAMA Network experience by selecting one or more topics from the list below.
Create a personal account or sign in to: